Civil Engineering ► Engineering Materials ► Tests on Bitumen Asphalt
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Experience in using bitumen in engineering projects has led to the adoption of certain test procedures that are indicative of the characteristics that identify adequate performance levels. Some of the tests have evolved with the development of the industry and are empirical methods. Consequently it is essential that they are carried out in strict compliance with the recommended procedures if they are to be accurate measurements of the bitumen's properties.
1. Penetration Test
2. Flash Point Test
3. Solubility Test
4. Ductility Test
5. Viscosity Test
Test 1. Penetration Test on Bitumen
The penetration test is one of the oldest and most commonly used tests on asphalt cements or residues
from distillation of asphalt cutbacks or emulsions. The standardized procedure for this test can be found
in ASTM D5 [ASTM, 2001]. It is an empirical test that measures the consistency (hardness) of an asphalt
at a specified test condition.
Procedure of Penetration Test on Bitumen:
In the standard test condition, a standard needle of a total load of 100 g is
applied to the surface of an asphalt or Liquid bitumen sample at a temperature of 25 °C for 5 seconds. The amount of
penetration of the needle at the end of 5 seconds is measured in units of 0.1 mm (or penetration unit).
A softer asphalt will have a higher penetration, while a harder asphalt will have a lower penetration.
Other test conditions that have been used include
- 0 °C, 200 g, 60 sec., and
- 46 °C, 50 g, 5 sec.
The penetration test can be used to designate grades of asphalt cement, and to measure changes in
hardness due to age hardening or changes in temperature.
Read a detailed procedure of Bitumen Penetration Test with Sample Data
Test 2. Flash Point Test on asphalt:
The flash point test determines the temperature to which an asphalt can be safely heated in the presence
of an open flame. The test is performed by heating an asphalt sample in an open cup at a specified rate
and determining the temperature at which a small flame passing over the surface of the cup will cause the
vapors from the asphalt sample temporarily to ignite or flash. The commonly used flash point test methods
include
- The Cleveland Open Cup (ASTM D92)
- Tag Open Cup (ASTM D1310).
The Cleveland
Open-Cup method is used on asphalt cements or asphalts with relatively higher flash points, while the
Tag Open-Cup method is used on cutback asphalts or asphalts with flash points of less than 79 °C.
Minimum flash point requirements are included in the specifications for asphalt cements for safety
reasons. Flash point tests can also be used to detect contaminating materials such as gasoline or kerosine
in an asphalt cement. Contamination of an asphalt cement by such materials can be indicated by a
substantial drop in flash point.
When the flash point test is used to detect contaminating materials, the
Pensky-Martens Closed Tester method (ASTM D93), which tends to give more indicative results, is
normally used. In recent years, the flash point test results have been related to the hardening potential
of asphalt. An asphalt with a high flash point is more likely to have a lower hardening potential in the field.
Read a detailed procedure of Bitumen Penetration Test with Sample Data
Test 3. Solubility Test on asphalt bitumen
Asphalt consists primarily of bitumens, which are high-molecular-weight hydrocarbons soluble in carbon
disulfide. The bitumen content of a bituminous material is measured by means of its solubility in carbon
disulfide.
Procedure for Solubility test on Bitumen
In the standard test for bitumen content (ASTM D4), a small sample of about 2 g of the asphalt
is dissolved in 100 ml of carbon disulfide and the solution is filtered through a filtering mat in a filtering
crucible. The material retained on the filter is then dried and weighed, and used to calculate the bitumen
content as a percentage of the weight of the original asphalt. Due to the extreme flammability of carbon disulfide, solubility in trichloroethylene, rather than
solubility in carbon disulfide, is usually used in asphalt cement specifications. The standard solubility
test using trichloroethylene is designated as ASTM D 2042.
The solubility test is used to detect contamination in asphalt cement. Specifications for asphalt cements
normally require a minimum solubility in trichloroethylene of 99.0 percent.
Unfortunately, trichloroethylene has been identified as a carcinogen and contributing to the depletion
of the earth’s ozone layer. The use of trichloroethylene will most likely be banned in the near future.
There is a need to use a less hazardous and non-chlorinated solvent for this purpose. Results of several
investigations have indicated that the solvent n-Propyl Bromide appears to be a feasible alternative to
trichloroethylene for use in this application.
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Test 4. Ductility Test on Asphalt
The ductility test (ASTM D113) measures the distance a standard asphalt sample will stretch without
breaking under a standard testing condition (5 cm/min at 25 °C). It is generally considered that an asphalt
with a very low ductility will have poor adhesive properties and thus poor performance in service. Specifications for asphalt cements normally contain requirements for minimum ductility.
Read a detailed procedure of Bitumen Penetration Test with Sample Data